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Document / 13 pages

GCMS analysis results for sample AD24700, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24700 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068880–000068892

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068889
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File t C:\HPCHEM\1\DATA\NOV0501\24700.D vial: 21 Acq On : 6 Nov 2001 7:27 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.41 ug/1 64513 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan)2rI 102 C6H140 000626-93-7 83 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-Butanol, 3-methyl- 102 C6H14O 000565-60-6 50 4 ,3^eptanol 116 C7H16O 000543-49-7 39 Nsurftlance Scan 177 (6.666 min): 24700.D (-) m/z 44.95 100.00% 4)5

5000

41 69 ■ ' ‘ ‘ . I I ■ I . . I I I . I

49 56 I 6.40 6.60 6.80 7.00 38,. I' > I ■ > I' I > 11 ■ 11 “ ■ 1 > 11111 ... . ...................... ■ I' < • • 1 • • I) I' I" I" >' I' Wz 41.00 19.96% nyz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1792:2-Hexanol 4)5

5000 6.^I 6.60 6.80 7.00 m/z 69.05 17.63% 39 42, ^58 84 87 ■ 11"' 11' I • 11 • I 11 I I i-r( 11 I 11 I I I. I I I I I I I I I I I I I I I I I I 11 I 11 I I I I I I I 11 I 'nA:-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63547:2-Pentanol. 4-methyl- 4)5 A 6.40 6,60 6.80 7.00 5000 m/z 43.05 10.82%

■nfe-> Abundance 20 m-p. X 27 69 I ' 1 ’' ‘ ‘ T ‘ 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 84 87 57 1 • * ‘ * 1 ‘ ‘ ‘ ‘ 1 * ’

#1777:2-Pentanol. 3-methyl- 4|5 ’ * I ‘H

“mTz L ‘ " 6.40 ' ‘ 6.^ " 6JO " 7.00 " ' 44.00 10.28% 5000

41 27

■nfe-> ' I'''' I' 20 25 ‘ I *''' 1' 30 35 40 45 .,,?X..... ................ ,,, 50 55 W 65 70 TO 80''as 90 6.40 6.a " aw " 7.66

24700.D NP103001.M Tue Nov 13 12:09:16 2001 Page 2

NYC-WTC_000068889

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NYC-WTC_000068889Source: NYC Law Department, mirrored locally

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