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GCMS analysis results for sample AD24700, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24700 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068880–000068892

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24700.D Vial: 21 Acq On : 6 Nov 2001 7:27 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.73 ug/1 116716 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 Oxiran^< 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 3 2-He;j^none, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Mebh;[yl Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance Scan 150 (6.418 min): 24700.D (-) m/z 42.95 100.00% 43

58 5000

71 85 100 6.00 6.20 6.40 6.60 6.80 I I m/z 58.05 57.85% T’’ Tife-> 20 30 50 60 70 80 90 ioo' iw' w '146 Abundance #1556:2-Hexanone 43

58 5000 I I r. . I I i'^ . I ' 6.00 6.20 6.40 6.60 6,80 m/z 57.00 17772% 71 85 1M I........... . ................................................................................................. ,

TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane, 2-methyl-2-(1-m^ylethyI)- 43 58 6.66 ' 6.20 6.^' 6.^ RTO 5000 “m/z 41.00 12.10% 71 85 100 I Tife-> '20'' ‘ i" ‘ '40' '1 ' ' I ‘ 1 ‘ ' I ' 50 60 70 80 M "ioo' iio' '126' im' '146 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43 6.00 6.20 6.40 6.60 6.80 58 m/z 100.0511.47% 5000

iiZz-> 29

' I'''' i ‘ 20 30 71 I ' I ‘ ‘ ‘' I' ‘ ‘' I'''' I' 40 50 60 70 m '' '96' "ioo "i-io' 'w 130 140 /I n A 6.00 6.^ k 6.40 6.60 6.80

24700.D NP103001.M Tue Nov 13 12:09:13 2001 Page 1

NYC-WTC_000068888

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NYC-WTC_000068888Source: NYC Law Department, mirrored locally

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