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GC/MS analysis results for sample AD22776, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22776 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087670–000087681

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22776.D Vial: 13 Acq On : 3 Oct 2001 1:51 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 6.48 0.96 ug/1 117876 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 intative ID MW MolForm CAS# Qual

1 2-Hexanonj 100 C6H12O 000591-78-6 91 2 Oxirane, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 3 2-Hexa: me, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Methy: Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance / Scan 157 (6.479 min): 22776.D (-) m/z 42795 100.00% 43

58 5000

85 100 AJ 71 __a20__640__6J50_6JBg__ I, I , . ...... |l|l|l| 51. , I , I, ,1 m/z 58.05 58.18% Ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 5000 ' ' I ' ' ' ' I ' ' ' ' I ' 6.20 6.40 6.60 6.80 m/z 56.95 18.02% 27 71 85 100 I, I , , ,1,........ |l L tVz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530; Oxirane, 2-methyl-2-(1-methylethyl)- 43 58 6.20 6.40 6.60 6.80 553 m/z 41.05 14.54% 71

30 85 100 ' I' '' ' I''' ' H 'i ' ' I ' I ' ' I ' ' I '' ' 'I '' ' ' I' ' ' 'I ' ' ''I '' ''I ‘ TT/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43 __a20_640_a60__a80^_ m/z 99795 11.17% 58 5000 29

' I ‘ ‘ ' ' I I ' ' ' I I ,1, ' I ' ' ' ' I ' 71 85 100 , |1, , , , I , A , I , , , , . 140 Tl/Z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

22776.D NP091101.M Thu Oct 04 14:27:13 2001 Pa OP 2

NYC-WTC_000087677

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NYC-WTC_000087677Source: NYC Law Department, mirrored locally

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