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GC/MS analysis results for sample AD22776, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22776 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087670–000087681

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087678
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT0201\22776.D Vial: 13 Acq On : 3 Oct 2001 1:51 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.45 ug/1 55372 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual

1 3-He^nol 102 C6H14O 000623-37-0 83 2 3-P^tanol 88 C5H12O 000584-02-1 42 3 3-^ntanol, 2-methyl- 102 C6H14O 000565-67-3 39 4 4-/ieptanol 116 C7H16O 000589-55-9 14 ^bundai Scan 172 (6.617 min); 22776.D (-) m/z 59705 100.00% 5b

5000 73 43 ..... .... 84 6.20 6.40 6.60 6.80 7.00 "' I'"' I" " I" " I . ..... Il.. ........... ... Wz 55.00 77.73% Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63527:3-Hexanol 5^

5000 73 1'1'' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ 31 6.20 6.40 6.60 6.80 7.00 m/z 73.00 44.55% 45 4# ............. ..... . 84 r Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Waundance #62941:3-Pentanol 5)9

31 6.20 6.40 6.60 6.80 zoo 5000 m/z 43.00 27.24% 41

. ...?^,|l,np,,l|lu.| 87 Tife-> Abundance t 1'“ ' I" "T 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #63561:3-Pentanol, 2-methyl- 5)9 I " '' I' " ' 1'''' I r

6.20 AJ 6.40 6.60 6.80 7.00 m/z 41.00 22.09% 5000 73

31 45 85 Tt+4- U I " ‘'I 102 i""i v ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

22776.D NP091101.M Thu Oct 04 14:27:15 2001 Paae 3 NYC-WTC_000087678

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NYC-WTC_000087678Source: NYC Law Department, mirrored locally

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