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GC/MS analysis results for sample AD22776, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22776 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087670–000087681

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087679
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22776.D vial: 13 Acq On : 3 Oct 2001 1:51 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) ' Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★if******* Peak Number 4 2-Hexanol Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.52 ug/1 64432 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual

1 2-Hex^ol 102 C6H14O 000626-93-7 83 2 2-PerU:anol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-Hekanol, (S)- 102 C6H14O 052019-78-0 64 4 2-Butanol 74 C4H10O 000078-92-2 50 Abundance/ Scan 184 (6.727 min): 22776.D (-) m/z 44.95 100.00% 40

5000

41 69 49 SB 84 87 6.40 6.60 6.80 7.00 I'''' I ' ''' I'''' I'''' [ ,.?flll,ll +rrtp-,Tr|4+tTTrrTTrr '■'h 11IIIIIII11 m/z 69700 17.20% TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584:2-Hexanol 40

5000 6.40 6.60 6.80 m/z 41.05 k 7.00 13.70% 19 2/31 4^1 8487 56 ......... . r TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546: 2-Pentanol, 4-methyl- 4b

6.40 6.60 6.80 7.00 5000 m/z 42.95 12.26%

27 69 19 I 31 57 42 8487 ' I'''' I' " Ii-i-l I |||||'||'|ll'|| 'n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769: 2-Hexanol, (S)- 40 6.40 6.60 6.80 7.00 m/z 43.95 8.00%

5000

55 8487 " I • • 111 • I " I " 11111111 •" 11" 111 ■ 111111" I " • • 11 Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22776.D NP091101.M Thu Oct 04 14:27:17 2001 Paae 4 NYC-WTC_000087679

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NYC-WTC_000087679Source: NYC Law Department, mirrored locally

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