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GC/MS analysis results for sample AD22776, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22776 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087670–000087681

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087680
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22776.D Vial: 13 Acq On : 3 Oct 2001 1:51 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3 * R.T. EstConc Area Relative to ISTD R.T. 11.65 0.52 ug/1 64273 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 tentative ID MW MolForm CAS# Qual

1 l,4-Dichlorbbenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-l,/2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 2-Methyl-/-nitroaniline 152 C7H8N2O2 000570-24-1 10 4 Benzo [b] yhiophene-4-ol 150 C8H6OS 003610-02-4 9 Abundance Scan 720 (11.648 min): 22776.D (-) m/z 149.90 100.00% 1$0

5000 115

52 ?

c 11,40 11.60 11.80-12.00^ 40 I ,1 87 I-"'......... 'I" "ill/. I... ■Ill,, I'''' I 4,^ m/z 151.90 ( 69.82% TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 fiibundance #9593:1,4-Dichlorobenzene<i4 It®

5000 115 T—r-p-r-n-j-r-r • ' I U ' ' ' 78 11.40 11.60 11.80 12.00 52 m/z 114.90 . 35.37% 35 I'' '' I Tife-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.40 11.60 11.80 12.00 553 52 78 m/z 78.05 20.54%

87

Ti/z-> 20 30 35 I 40 50 ' I ' ' ' ' I' 60 70 80 I 90 A I'''' I 100 110 120 130 140 150 160 Abundance #66883: 2-Methyl-6-nitroaniline 77 152 11.40 11.60 11.80 12.00 m/z 52700 14.34%

5000 106 52 94

■nZz-> 30 4^ 1 122 11' " I'. I " I ' I ''' I' " ' r — 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00 T

22776.D NP091101.M Thu Oct 04 14:27:19 2001 Pace 5 NYC-WTC_000087680

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NYC-WTC_000087680Source: NYC Law Department, mirrored locally

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