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GCMS analysis results, sample AD23909, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067555–000067578

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23909.D vial: 4 Acq On : 18 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.73 0.68 ug/1 64008 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hex^ol 102 C6H14O 000626-93-7 83 2 2-Pe?(tanol, 4-methyl- 102 C6H14O 000108-11-2 83 3 2-^ntanol, 3-methyl- 102 C6H14O 000565-60-6 40 4 2/Butanol 74 C4H1O0 000078-92-2 39 iggmiaice Scan 184 (6.728 min): 23909.D (-) m/z 45.05 100.00% 4|5

5000

69 . I I n ' ‘ I ' ' ' ' I ' ' ' ' I ' ‘ ' I 8487 6.40 6.60 6.80 7.00 ........ ....................................... m/z 69.00 18.76% Tlfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63583:2-Hexanol 4^

5000 t4 6.40 6.60 6.80 7.00 m/z 43.05 14.91% 69 ^58 I 8487 Tn1-tltiiuiiiii.l|i..i|iinyrn-r|iliiiiuiii 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63545:2-PentanoI, 4-iTi8thyl-

5000 4(5 J 6.40 m/z 6.60 6.80 7.00 13.84%

69 27 3942 , 57 Tlfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 . I,.. .... ^bundance #63555:2-Pentanol, 3-methyl- 4|5 6.^ 6.60 6.80 7.00 ra/z 44.00 9.97% 5000

TiZz-> 5 56 53,1, 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 69 87 6.40 6.60 I 6.80 7.00

23909.D NP101901.M Tue Oct 23 14:32:32 2001 Page 4 NYC-WTC_000067575

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NYC-WTC_000067575Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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