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GC/MS analysis results for sample AD22914, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22914 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087540–000087561

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCTO 2 01\22914.D vial: 4 Acq On 2 Oct 2001 5:03 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.53 ug/1 64832 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual

1 2-He: .nol 102 C6H14O 000626-93-7 83 2 2-P^ •tanol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2- ;xanol, (S) - 102 C6H14O 052019-78-0 43 4 2 eptanol 116 C7H16O 000543-49-7 40 ^bund^ce Scan 185 (6.739 min): 22914.D (-) m/z 44795 100.00% 4b

5000-

41 84 87 6.40 6.60 6.80 7.00 in/z 69710 16.39% TVk-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 <\bundance #63584: 2-Hexanol 4b

5000 .......... "I'..... 'I 6.40 6.60 6.80 7.00 69 m/z 41.05 14.78% 19 27 31 4^1 tVz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 . I........ 75 80 85 90 95 Abundance #63547:2-Pentanol, 4-methyl- 4b 6.40 6.60 6.80 7.00 5000 m/z 43.00 13.65%

27 ■38.-^ 57 8487 Tl/Z-> 10 I 15 'I 20 X 25 30 T 35 40 -tT-nrp-TT-rrH-rTp-rrTp-r^^ 45 50 55 60 65 70 75 80 85 90 95 /Kbundance #1769; 2-Hexanol, (S)- 4b 6.40 6.60 6.80 7.00 m/z 44.00 11.58%

5000

55 8487 " ' I • • " I •' " I " "I " 111 ■ IIII, " . 11 n 1111,.,, " 11. Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22914.D NP091101.M Wed Oct 03 09:48:57 2001 Page 3

NYC-WTC_000087549

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NYC-WTC_000087549Source: NYC Law Department, mirrored locally

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