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GC/MS analysis results for sample AD22914, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22914 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087540–000087561

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087550
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT0201\22914 .D Vial: 4 Acq On : 2 Oct 2001 5:03 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 11.64 0.51 ug/1 62939 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual

1 1,4-Dj/chlorobenzene-d4 150 C6C12D4 003855-82-1 47 2 Benz^e-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 28 3 Acenaphthylene 152 C12H8 000208-96-8 9 4 Biphenylene 152 C12H8 000259-79-0 9 Abundance Scan 719 (11.641 min): 22914.D (-) m/z 149.90 100.00% 1!i0

5000 115 78 52 11.40 11.60 11.80 12.00 38 V I ''' ' I U- I '' ' ' I ... m/z 151.90 65.50% Tife-> Abundance 30 40 50 60 70 80 90 100 110 120 130 140 150 160 #9593:1,4-Dichlorobenzene-d4 (1 1!i0

553 78 115 .. A\. 11.40 11.60 11.80 12.00 52 m/z 115.00 39.44%

■n^-> 30 35 40 50 ' I ' UUn ■ I ' I • 11 • • I 60 70 80 90 100 110 120 130 140 150 160 .... Abundance #9592: Benzene-1,2,3,4-d4-, 5.6-dichloro- 1!i0

115 11.40 11.60 11.80 12.00 553 52 78 m/z 78705 22.62%

35 87 I I ’ I' ’ ' ' I ' 11 • • • • I • • • • I • n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67015: Acenaphthylene i;i2 11.40 11.60 11.80 12.00 m/z 52.00 . 14.80% 553

87 98 126 '' I'''' I'''' I'''' I'' I' I'''' I'''' I II I ■n/2-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

22914.D NP091101.M Wed Oct 03 09:48:59 2001 Page 4

NYC-WTC_000087550

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NYC-WTC_000087550Source: NYC Law Department, mirrored locally

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