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GC/MS analysis results for sample AD22916, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22916 conducted on October 5, 2001, noting other unknown compounds.

NYC-WTC_000087575–000087585

Folder label: “GC/MS Scan 9/20/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0201\22916.D Vial: 6 Acq On : 2 Oct 2001 7:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.64 0.54 ug/1 66964 1,4-Dichloroberizene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-D3^hlorobenzene-d4 150 C6C12D4 003855-82-1 50 2 Benze/e-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 Biph/nylene 152 C12H8 000259-79-0 9 4 Acenaphthylene 152 C12H8 000208-96-8 9 Sundance. Scan 719 (11.642 min): 22916.D (-) m/z 149.90 100.00% 1!i0

5000 115

52 ” 11.40 11.60 11.80U~2W Ti/z-> 30 Ui. 40 50 60 70 80 90 100 110 120 130 140 150 160 m/z 151.90 I'''' I '65.15% Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 78 11.40 11.60 11.80 12.00 52 m/z 115.00 40.84% 35 T-p- JU.... ■nk-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1ii0

115 11.40 11.60 11.80 12.00 5000 52 78 m/z; 78.05 22.19%

35 87 ......... ' I' ' ' ' r I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' JU.... tVz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #67017: Biphenylene 152 11.40 11.60 11.80 12.00 m/z 52.00 15.42%

5000

63 76 97 ^26 ' i'''' I'''' I' ' I ' '' ' I ' ' ''''I I ' ' ' I ' ' ' ' I I ' I ' I ' n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.40 11.60 11.80 12.00

22916.D NP091101.M Wed Oct 03 10:06:13 2001 Page 1

NYC-WTC_000087583

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NYC-WTC_000087583Source: NYC Law Department, mirrored locally

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