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GCMS analysis results for sample AD24640, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24640 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068659–000068671

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068668
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0501\24640.D Vial: 13 Acq On 5 Nov 2001 11:40 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.42 ug/1 67872 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanol/^ 102 C6H14O 000626-93-7 83 2 2-Pentax^, 4-methyl- 102 C6H14O 000108-11-2 64 3 2-Hexefnol, (S) - 102 C6H14O 052019-78-0 43 4 2-P^tanol, 3-methyl- 102 C6H14O 000565-60-6 40 Abundance Scan 177 (6.667 min): 24640.D (-) in/z 44795 100.00% 4|5

5000

69 ' ' ' 'T'" 39 I 55 6.40 6.60 6.80 7.00 I........ ........................... "I I... Xl...... m/z !69.00 19.59% nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63583: 2-Hexanol 4(5

5000 6.40 6.60 6.80 7.00 “m/z 41705 18.63% 69 39 55 ...... ‘"I...... Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63546:2-Pentanol. 4-methyl- 4(5

6.40I 6.60 6.80 7.00 5000 m/z 43.00 12.84%

27 69 57 I . infe-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105

4(5 #1769:2-Hexanol. (S)- I'" 11" " I" " I'" 11' I" I I" " I JM 6.40I 6,60 6.80 7.00 m/z 43.95 7.99% 5000

55 ? 87 " I" " I ‘ ‘" I" ‘ h " " I'"' I I" " I" ‘' I TTfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 7.00

24640.D NP103001.M Fri Nov 09 12:25:40 2001 Page 2

NYC-WTC_000068668

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NYC-WTC_000068668Source: NYC Law Department, mirrored locally

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