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GC/MS analysis results for sample AD22579, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087180–000087201

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22579.D Vial: 7 Acq On : 28 Sep 2001 6:18 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Hexanol Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 6.75 0.54 ug/1 77032 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual

1 2-H^anol 102 C6H14O 000626-93-7 78 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 78 3 2-Hexanol, (R) - 102 C6H14O 026549-24-6 40 4 2/Hexanol, 3-methyl- 116 C7H16O 002313-65-7 39 ^bund^nce Scan 187 (6.755 min): 22579.D (-) m/z 44.95 100.00% 4)5

5000

41 69 53^1^59 65 1 72 640 6,60 6.80 7.00 Srl+U m/z 68.95 15.92% Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584: 2-Hexanol 4)5

A 5000 tA 640 6.60 6.80 7.00 69 m7z 41.05 13.58%

Tl/Z-> Abundance 19 ....... . 56 8487 ■ I " 111111 > I ■ I " I' 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #63546:2-Pentanol, 4-methyl- a 43 I ' 640 6,60 6.80 7.00 5000 m7z 42.95 10.35%

27 69 19 I 31 4; I 8487 "I......... . .............. * I " ’' 111 " I •''' I • * H I.. 111.11.1.1111.1.. J111 111 Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance! #1794:2-Hexanol. (R)- 43 6.40 6.60 6.80 7.00 m/z 44.00 9.15%

5000

69 55 ' " I' ■ 111 ■ ■ ■ ■ I' ■ ■ ■ I 84 87 '' I'' ‘' I' mZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6,40 6,60 6.80 7.00

22579.D NP091101.M Tue Oct 02 11:50:07 2001 Page 3

NYC-WTC_000087189

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NYC-WTC_000087189Source: NYC Law Department, mirrored locally

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