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GC/MS analysis results for sample AD22578, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22578 conducted on October 10-11, 2001, identifying unknown compounds.

NYC-WTC_000087163–000087179

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087173
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NYC 9/11 Public Portal Document

Library Search Compound Report 'Data File : C:\HPCHEM\l\DATA\SEP2801\22578.D Vial: 6 Acq On : 28 Sep 2001 5:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 6.75 0.67 ug/1 90010 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexani 102 C6H14O 000626-93-7 83 2 2-Pent .ol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-He Zanol 116 C7H16O 000543-49-7 50 4 2-Hl anol, 3-methyl-________________ 116 C7H16O 002313-65-7 45 ^bundanc^ Scan 187 (6.754 min): 22578.D (-) m/z 44.95 100.00% 4^

5000 ; 69 51 56 6 40 6.60 6.80 7.00 11 " 111" 1 m/z 68.95 17.29% Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1792:2-Hexanol 45

5000 6 40 6,60 ■ 6,80 7.00 "mTz 40795 16.75% 27 39 55 69 87 TTfVrTTf+t+TT I' " ' I " '' I Ti/z-> 20 25 30 35 40 -45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63545: 2-Pentanol, 4-methyl- 4

_64Q__a60_a80_7;0g^__ 5000 m/z 43.00 11.08%

69 57 ' I''' L"" I"" I 87 ....... 'I%ll 111II >1111111111 I'''' I ‘' I n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #64346: 2-Heptanol 43 640 6.60 6.80 7.00 "m/z 43.95 9.67% 5000

27 55 I 39 ................ |ll"|ii'i| 70 83 101 III111 il 11 |i I n I I I 11 I 111 I

nZz-> . .... 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.40 6.60 6.80 7.00

22578.D NP091101.M Wed Oct 03 11:30:01 2001 Page 4 NYC-WTC_000087173

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NYC-WTC_000087173Source: NYC Law Department, mirrored locally

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