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GCMS analysis results for sample AD24483, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24483 identifying unknown compounds on November 13, 2001.

NYC-WTC_000068763–000068777

Folder label: “GCMS Scan X 10/15/01 A 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24483.D Vial: 22 Acq On : 3 Nov 2001 11:26 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.55 0.64 ug/1 96065 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexani 102 C6H14O 000623-37-0 74 2 3-Penta': 2-methyl- 102 C6H14O 000565-67-3 38 3 3-Penta: 88 C5H12O 000584-02-1 36 4 2-Pr9^panol, 2-methyl- 74 C4H10O 000075-65-0 33 Abundance Scan 164 (6.552 min): 24483.D (-) m/ z 59.00 100.00% 5^

5000 73 43 ' I ' ' ' ' I 51 6 20 6.40 6.60 6.80 I'''' I -T-+T I" " I" " I" " I" " I" " I m/z 55700 76.51% Ti/2-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63531:3-Hexanol 5(3

5000 73 54 6.20 6.40 6.60 6.80 43 m/z 73.00 44.27%

+t +t 44 -f+ T I'"' I"'' I

L ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561:3-Pentanol, 2-methyl- 5(9

6.20 6.40 6.60 6.80 5000 73 m/ z 42.95 27.42% 31 45 85 102 n/z-> Abundance "'I""I"' . ... I'' " I " " I' I" " I 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #62941:3-Pentanol 5(9 620 AJ 6.40 6.60 6.80 m7z 41700 20.86% 31 5000

41 ... I|llli| 87 I" " I I"'' I''" I''" I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80

24483.D NP103001.M Fri Nov 09 15:03:11 2001 Page 3

NYC-WTC_000068773

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NYC-WTC_000068773Source: NYC Law Department, mirrored locally

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