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GCMS analysis results for sample AD23998, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23998 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067796–000067810

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\23998.D Vial: 6 Acq On : 25 Oct 2001 5:35 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : .C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.61 0.43 ug/1 87692 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 / Tentative ID MW MolForm CAS# Qual 1 3-Hexano' 102 C6H14O 000623-37-0 83 2 3-PentaHj 88 C5H12O 000584-02-1 42 3 2-Pro^ni 2-methyl- 74 C4H10O 000075-65-0 40 4 3-HepXan< 116 C7H16O 000589-82-2 36 Abundance < Scan 170 (6.605 min): 23998.D (-) m/z 59705 100.00% 50

5000 73 43 6.20 6.40 6.60 6.80 7.00 3? , I, 48 4 m/z 54.95 83.72% iiZz-> Abundance 10 20 30 40 50 60 70 #63529:3-Hexanol 80 90 100 110 1

5000 31 73 6.20 6.40 6.60 6.80 7.00 m/z 7^700 45.51% 44 . I'l'.-ri. 4;l‘l ' ■ ■ ' I I ' I ' ■ ■ ‘ I ‘ 102 ‘ ' I ‘ ' I nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #82943:3-Pentanol 50 6.^ ' ' 6.^ ' ‘ 6.^*^"^6.^ ' ‘ 7.00' 31 5000 m/z 43700 28.33% 41

4' I'''' I'' ‘' I ' ‘ ' I ■ ■ ‘ ‘ I ‘‘ I Tife-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62575:2-PropanoI. 2-methyl- I I . , . I .... I , I 6.20 6.40 6.60 6.80 7.00 “m/z 41705 20.42% 5000 31 41 15 2# ' I ' ' ' ' I ‘ ‘ I ' ' ' ' I ' ' ' ' 1 ' ‘ ‘ I ■nfe-> 10 20 30 40 50 60 70 80 90 IO) 110 6.20 6.40 6.60 6.80 7.0)

23998.D NP101901.M Fri Oct 26 10:12:21 2001 Page 3

NYC-WTC_000067806

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NYC-WTC_000067806Source: NYC Law Department, mirrored locally

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