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GC/MS analysis results for sample AD22578, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22578 conducted on October 10-11, 2001, identifying unknown compounds.

NYC-WTC_000087163–000087179

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087172
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22578.D vial: 6 Acq On : 28 Sep 2001 5:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************************************************************************** Peak Number 3 3-Hexanol Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 6.64 0.43 ug/1 58268 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexanj 102 C6H14O 000623-37-0 86 2 Oxepa: A, 2,2,3-trimethyl- 100 C6H12O 023120-43-6 64 3 3-Pe; tanol 88 C5H12O 000584-02-1 40 4 3-P^ tanol, 2-methyl-_______________ 102 C6H14O 000565-67-3 39 ^bundanc^ Scan 175 (6.644 min): 22578.D (-) m/z 59.05 .100.00% 5(9 55

73 43 RQ 6,40 6.60 6,80 7.00 . 49 81 86 100 p-myn-n-r TTTrlrW+tTTT+T+rtT tt+tt+t+t m/z 55.00 78.51% t:/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63531:3-Hexanol 5b

5000 73 6.40 6.60 6,80 7.00 43 m/z 73.00 44.69% i"'i|"li|......... +4 I'............ ' I “'' I' " ' I'''' I' " ' I' " ' I'''' I'' " I TT/z-> 20 25 30 35 40,45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1518: Oxepane, 2,2,3-trimethyl- 5(9 , , ri I . M . I , 4V7Y1 . , I *, . 42 6.40 6.60 6.80 7.00 5000 m/z 43.05 24.78% 70 27 53 p-n-rp-r+r +t+ ...... ■nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62942:3-Pentanol 5b __^_a40__a60_e8gL_7;00_ “m/z 41.05 23.20% 31 5000

41

tHh|I......... . .......... 87 I'' " I I "" I • H 11 .... I .... I Tl/Z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.40 6.60 6.80 7.00

22578.D NP091101.M Wed Oct 03 11:29:59 2001 Page 3 NYC-WTC_000087172

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NYC-WTC_000087172Source: NYC Law Department, mirrored locally

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