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GC/MS analysis results for sample AD23473, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.

NYC-WTC_000088725–000088752

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C;\HPCHEM\1\DATA\OCT1601\23473.D Vial: 4 Acq On : 16 Oct 2001 5:10 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************************************************************************ Peak Number 3 3-Hexanol Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.41 ug/1 39992 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Hexanyi 102 C6H14O 000623-37-0 90 2 Oxi ran/, tetramethyl- 100 C6H12O 005076-20-0 50 3 3-Ocenol 130 C8H18O 000589-98-0 50 4 Oxepane, 2,2,3-trimethyl-___________ 100 C6H12O 023120-43-6 45 Abundance Scan 172 (6.617 min): 23473. D (-) m/z 59.00 100.00% 55

5000 43 73

6.20 6.40 .J',. 6.60 6.80 7.00 84 100 207 . ............... I" " I " " I “ " I f'''' I m/ z 55.00 84.57% Ti/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #63531: 3-Hexanol 55

5000 73 6^ 6.20 6.60 6.80 7.00 43 m/z 73.00 47.50% WtTTTTT^ ....... ....... jTTTTpTTTpTTTyrrTTpTTTyrTTTp-rrrpT-rrpT^^ Tl/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance__ —#63415: Oxirane, tetramethyl- 59 43 -.......................... I

6.20 6.40 6.60 6.80 7.00 m/z 27.42%

85 100 tVz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 Abundance #65311:3-Octanol T 55 6.20 6.40 - 6.60-- 6.80 7.00 m/z 41.00 18.25% 83 5000

101 45 72 h 112 TT/z-> ......... W| I'............. TtTTT ■Yrrrrp-rrr^TTTTYrrrr^TTTTp-rrr^^ 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 200 210 6.20 6.40 6.60 6.80 7.00

23473.D NP091101.M Wed Oct 17 13:17:28 2001 Page 3

NYC-WTC_000088734

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NYC-WTC_000088734Source: NYC Law Department, mirrored locally

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