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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088216
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 19 R.T, EstConc Area Relative to ISTD R.T. 6.62 0.46 ug/1 42455 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexane^ 102 C6H14O 000623-37-0 83 2 Oxiran^ tetramethyl- 100 C6H12O 005076-20-0 59 3 3-Hep^nol 116 C7H16O 000589-82-2 39 4 2-Propanol, 2-methyl- 74 C4H10O 000075-65-0 38 Abundance' Scan 173 (6.625 min): 23320.D (-) Wz 59705 107700% 50

73 5000

41 “t ' '-I ' ' ' 6.20 6.40 6.60 6.80 7.00 85 i'''' I 4+ I................ I'' '' I'''' I' 100 ('"' I.’" u " " r "' I "mT^ 55.00 72.73% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63527: 3-Hexanol 50

5000 73 31 6.20 “ 6.40 6.60 6.80 7.00 m/z 73.00 49.18% 45 84 I I I■ ■ ■I 1 1 ,1 I , , ■ ■ I i I I . I■ 1 " I " ■.I ,., I I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63415: Oxirane, tetramethyl- 59 43 —— _6,20a40_a60__a80__7W_ 5000 m/z 41.05 24.60%

53 I 85 100 I'''' I''' * I ijrrrTTTrtrlTl- .................... I' • ’' I TrfTT Ti/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 V— Abundance #64384:3-Heptanol 59 6.20 6.40 6.60 6.80 7.00 69 m/ z 43.05 19.80% 41 5000 87

n/z-> I' ‘ " I hrrrr 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 98 I " " I 6.20 AJ 6.40 6.60 6.80 7.00

23320.D NP091101.M Mon Oct 15 09:53:36 2001 Page 3

NYC-WTC_000088216

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NYC-WTC_000088216Source: NYC Law Department, mirrored locally

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