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GC/MS analysis results for sample AD22578, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22578 conducted on October 10-11, 2001, identifying unknown compounds.

NYC-WTC_000087163–000087179

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087171
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NYC 9/11 Public Portal Document

Library Search Compound Report •Data File : C:\HPCHEM\l\DATA\SEP2801\22578.D Vial: 6 Acq On : 28 Sep 2001 5:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************** Peak Number 2 2-Hexanone. Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.51 0.85 ug/1 114453 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-HexMone 100 C6H12O 000591-78-6 91 2 2-He^none, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 52 4 Prppanal 58 C3H6O 000123-38-6 43 4bund%hce Scan 160 (6.506 min): 22578.D (-) m/z 43700 100.00% 43 A 58 5000

71 85 100 6.20 6.40 6.60 6.80

TiZz~> 20 30 40 igJU 50 60 -r^TTTTT/k-TTTTTTlr^^

70 80 90 , 100 110 120 130 140 m/z 58.05 57.72% Abundance #63387: 2-Hexanone 43

58 5000 6.20 6.40 6.60 6.80 100 m/z 57.00 16.22% 71 85 ' I ' ' ' ' I ' ' ‘ ''l I I I ' I ' ' ' ' I ' '' ' I ' Ti&-> 20 30 40 70 80 90 100 110 120 130 140 (Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.20 6.40 6.60 6.80 5000 29 "inTz 41.05 15.32%

Ti/z-> ‘'-I'--'‘''I ""I I' 20 30 40 50 X 60 70 71 I 80 85 . - 100 I ... . . 140 90 100 110 120 130 140 Abundance #63354: Methyl Isobutyl Ketone 43 _a20_640_a60_a8g^_ m/z 100.05 13.26%

5000 58 85 100 . I '“I ' ' ' 67 , I , I tVz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 a20 a40 6,60 6^

22578.D NP091101.M Wed Oct 03 11:29:57 2001 Page 2

NYC-WTC_000087171

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NYC-WTC_000087171Source: NYC Law Department, mirrored locally

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