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GC/MS analysis results for sample AD23319, Oct 15 2001

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Laboratory report documenting GC/MS analysis of environmental sample AD23319 conducted on October 15, 2001.

NYC-WTC_000088429–000088455

Folder label: “GC/MS Scan 9/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23319.D Vial: 21 Acq On : 12 Oct 2001 9:41 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 6.61 0.48 ug/1 46345 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hexan61 102 C6H14O 000623-37-0 83 2 3-Penfe(anol, 2-methyl- 102 C6H14O 000565-67-3 40 3 3-P^tanol 88 C5H12O 000584-02-1 33 4 4-9eptanol 116 C7H16O 000589-55-9 16 ^bundan^ Scan 171 (6.613 min); 23319.D (-) m/z 59.05 100.00% 5^

73

43 6.20 6.40 aeo 6.80 7.00 I'*"H 'i 4+ Wt I'' " I " ' ’ I' " ' I " '' I P" m/z 54795 78.26% ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63529: 3-Hexanol 519

31 5000 73 6.20 6.40 6.60 6.80 7.00 m/z 73.00 50.84% 44 102 tVz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63561: 3-Pentanol, 2-methyl- 5l9

6.20 6.40 6.60 6.80 7.00 73 m/^ 43.00 26.02% 31 45 85 102 4 TT/z-> 4bundance ....... tnTTTTT+pt ‘ i" " I " " I' " ' I " " I' " ' r ''' 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #62941:3-Pentanol 50 6.20 AJ 6.40 6.60 6.80 7.00 m/z 41700 25.06% 31 5000 41 87 TTrrrp-rrrr ■n&-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 6.20 6.40 6.60 6.80 7.00

23319.D NP091101.M Mon Oct 15 09:49:26 2001 Page 3

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NYC-WTC_000088438Source: NYC Law Department, mirrored locally

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