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GCMS analysis results, sample AD23909, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067555–000067578

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1801\23909.D Vial: 4 Acq On : 18 Oct 2001 7:07 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params; LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 3-Hexanol Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.62 0.51 ug/1 48181 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanolx 102 C6H14O 000623-37-0 83 2 3-Pentasol 88 C5H12O 000584-02-1 38 3 4-He]^nol 116 C7H16O 000589-55-9 12 ’ 4 l-Hppten-4-ol 114 C7H14O 003521-91-3 10 ^bundanc^ Scan 172 (6.618 min): 23909.D (-) m/z 59.05 100.00%

5000 73 41 6.20 ' ' 6.^ ' 6,^ ' 6^ ' 7.00 ' 4^I'l" " 11 80 90 ' ' 100 ' ' 110 m/z ^700 85.54% Ti/z-> 10 20 30 40 50 60 70 Abundance #63529:3-HexanoI 5|9

5000 31 73 6.20 6.40 6.60 6.80 7.00 m/^ 73.00 48.69% 44 102 ' • I ' ' ' ‘ I ' ' ‘ ' I ' >‘l " "t+ ' I ' • ‘ ‘ I ' ■ • ■ I ■ ' ' ‘ I TiZz-> 10 20 30 40 50 60 70 80 90 100 110 ^buruiance #62943:3-PentanoI 50 6.20 6.40 6.60 k 6.80 7.00 31 5000 m/z 41.00 30.37% 41

-‘''II I ' ' ' ' I ' ' ' ■ I ' ‘ ' I ‘ ‘ ' I ■ ‘ ‘ ' I TiZz-> 10 20 30 40 50 (60 70 80 90 100 110 Abundance #64376:4-Heptanol sis 6.20 6.40 6.60 6.80 7.00 73 m7z 437^5 16.89% 5000 43 27

10 ' '20' ‘ ■-r+ I'' ! ' I ‘‘ I ■ ■ ‘ ‘ I' ''' 1 ----- 1 I ■i-i-r-[ I I ■■ I I I I I I I •nZz-> 40 50 60 70 80 90 100 110 6.20 6.40 6.60 6.80 7.00

23909.D NP091101.M Fri Oct 19 10:17:06 2001 Page 3

NYC-WTC_000067565

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NYC-WTC_000067565Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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