GCMS analysis results, sample AD25495, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV1501\25495.D Vial: 3 Acq On : 15 Nov 2001 6:15 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.42 ug/1 74504 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexan(^e 100 C6H12O 000591-78-6 91 2 2-Hexa^one, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Oxira^ , 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 59 4 Methy/ Isobutyl Ketone 100 C6H12O 000108-10-1 50 Abundance Z Scan 151 (6.428 min): 25495.D {-) m/z 42.95 100.00% 4b

To,

51,1, 58

71 85 , ......... ,1, 100 .................. 6.00 m/z 6.20 w 58.00 6.40 6.60 6.80 52.72% m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556:2-Hexanone 4b

58 5000 6.00 6.20 6.40 6.60 6.80 m/z 41.05 20.09% 27 71 85 100 ,1, ' I ' ' ’ ' I ' m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43

58 6.00 6.20 6,40 6.60 6.80 5000 29 “m/z 57.00 13771%

mfe-> ' I ' ' ' ' I ' ' ' ' 11 20 30 40 ,1, ' I ' ' ' ' I ' 50 60 71 85 70 80 90 100 110 120 1“ 130 140 140 Abundance #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 600 6.20 6.40 6.60 6.80 58 ■m/z 38.95 8.90% 5000 71

30 85 100 ■ I ■ ■' ■ I > ■■ < I I I'''' I' I « . . '1’1 ' ' , m/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 elo 6.80

25495.D NP103001.M Wed Nov 21 12:43:28 2001 Page 1

NYC-WTC_000069705