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GCMS analysis results, sample AD25495, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD25495 conducted on November 26, 2001, noting unknown compounds.

NYC-WTC_000069697–000069707

Folder label: “GCMS Scan X 10/25/01 An 11/5/01

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Scanned page image, NYC-WTC_000069706
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\NOV1501\25495 .D Vial: 3 Acq On : 15 Nov 2001 6:15 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.16 ug/1 207488 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic a/id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Morphol0ie, 4-methyl- 101 C5H11NO 000109-02-4 9 4 1,3-Dio^olane-2-methanol, 2,4-dimet 132 C6H12O3 053951-43-2 9 Abundance Scan 289 (7.695 min): 25495.D (-) m/z 42.95 100.00% 4(3

59 5000

101 ~' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' 7.40 7.60 7.80 8.00 83 m/z 59.0.5 49.89% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275:2-Pentanone. 4-hydroxy-4-methyl- 4i3

5000 59 __L40__L60_^,80_8t0^_ m/z 100.95 22.03% 15 31 101 J..... I, I. I 83 I Ti^-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292; Acetic acid, 1,1-dimethylethyl ester 4(3 I ■ I I . I I ■ ( I > « I I . r I . I I < 7.40 7.60 7.80 8.00 5000 57 m/z 58.05 17.56% 101 15 27 I ' I ■ ' • ' I ' ■ ■ ■ I ' ■ ' I I I I • ■ I > ■ ■ I I ■ ■ ■ ■ ( nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640; Morpholine, 4-methyl- .. ' ' ' I ‘ ‘ 4|3 7.40 7.60 7.80 8.00 m/z 41.05 7.51%

tililil 101 15 1 I I ' ' ' ' \~ 27

40 , 56 1 Tlfe-> 10 20 30 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25495.D NP103001.M Wed Nov 21 12:43:29 2001 Page 2

NYC-WTC_000069706

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NYC-WTC_000069706Source: NYC Law Department, mirrored locally

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