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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089428
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23836.D Vial: 16 Acq On : 31 Oct 2001 5:09 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L A******************************************************************** Peak Number 4 2-Hexanol Concentration Rank 18 R.T. EstConc Area Relative to ISTD R.T. 6.67 0.54 ug/1 80677 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm. CAS# Qual

1 2-Hexaiy51 102 C6H14O 000626-93-7 78 2 2-Pentanol, 4-methyl- 102 C6H14O 000108-11-2 74 3 2-He:0nol, (S) - 102 C6H14O 052019-78-0 64 4 2-H^anol, (R) - 102 C6H14O 026549-24-6 43. Abundance ( Scan 178 (6.675 min): 23836.D (-) m/z 44795 100.00% 415

5000

I" " I" ” I" " I" " I 41 69 I.72 84^ eA 7o"75"8o"85 . m/z ' ' I ' ' 6.40 JU 6.60 69.00 6.80 7.00 15.86%

JL. TiZz-> 10 15 20 25 30 35 40 45 50 55 60 Abundance #1792:2-Hexanol

22 6.40 6.60 6.80 7.00 m/z 40.95 14.36% 27 5558 ® 8487 . .............. ll^J.... 3942 TpTTT-|-H-hp-rTTyrTT+pTTTYrTTTpTT-tYr+TTpT-TT^ ■nfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546:2-Pentanol, 4-methyl- ------ ---- ---------------------- --- _

u 6.40 6.60 6.80 7.00 5000 jn/z 44.00 11.99%

27 42 _ .57---------- ®iL_----------8487.-----

TVi;-> 10 15 20 25 30 35 Am 40 ■ I" " 111,. I ■... I,,, 11..,. I,,,, I," 11,1,,,,,,, I. 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769: 2-Hexanol, (S)- _4)5---------- i 6.40^-6,60“’ 6.80 7:00 ' m/z 43.05 11.93%

5000

TTTj!4rrTTp4X 55 ? M87-.'■ TTp-rrq-T I ■ ■ 111.. .1-p . I ■ I ■ ■ ■ 11111.1 ■ 1. 11. Ti/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 - 85 90 95 6.40 6.60 6.80 7.00

23836.D NP103001.M Thu Nov 01 13:27:03 2001 Page 4

' NYC-WTC_000089428 ’

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NYC-WTC_000089428Source: NYC Law Department, mirrored locally

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