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GC/MS analysis report, sample AD23699, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23699 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089158–000089170

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089169
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23699.D Vial: 12 Acq On : 15 Oct 2001 10:57 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.51 ug/1 47834 1,4-Dichlorobenzene-d4 11.77 Hit# Of 5 Tentative ID MW MolFdrm- CAS# Qual . 1 1,4-DichloroE)enzene-d4 150 C6C12D4 003855-82-1 53 2 Benzo [b] thwphene-4-ol 150 C8H6OS 003610-02-4 37. 3 Benzene-1 '2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 17. 4 Biphenyl^ e 152 C12H8 000259-79-0 9 <Kbundance Scan 717 (11.620 min): 23699.D (-) m/z 149.90 .100.00% 1!i0

5000 115 52 78 . ....................... 40 11.20 11.40 11,60 11,80 12.00 I , 63 TTrU+rpV m/z 151.90 60.95% n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 ^bundance #9593; 1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 36.60% 35 ' I ''' I' nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9645: Benzo[blthiophene-4-ol •liiO I ' ' ' ' I ' ' 121 11.20 11.40 11.60 11.80 12.00 5000 ■m/z 78.05 21.35%

. I 89--;|-————-I , TY<~'~rTyj-r-r-rYr-!‘-<^-\-ri-r-rYr-!‘^-rYrr-rTYr-r-r-r-^ T^ft-rn-n-r- Tife-> 30 40 50 60 . 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3,4-d4-. 5,6-dichloro- -1$0-T .1t20-11:40-11160 “11.80 ' 12.00- --m/'z—52-.-00 17T07% 115 5000 52 78

87

Tl/i-> 30 35 I 40 50 60 70 80 I A .................. /Jw I'''' I 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23699.D NP091101.M Tue Oct 16 15:11:01 2001 Page 4

NYC-WTC_000089i69

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NYC-WTC_000089169Source: NYC Law Department, mirrored locally

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