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GC/MS analysis report, sample AD23698, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23698 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089144–000089157

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089156
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1501\23698.D Vial: 11 Acq On : 15 Oct 2001 9:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.63 0.53 ug/1 50771 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-DichlorojDenzehe-d4 150 C6C12D4 003855-82-1 53 2 Benzene-1,2<3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 23 3 Benzenami/ie, 2-methyl-4-nitro- 152 C7H8N2O2 000099-52-5 14 4 BenzenaiFlne, 2-methyl-5-nitro- 152 C7H8N2O2 000099-55-8 10 ^bundance / Scan 717 (11.626 min): 23698.D (-) m/z 149.90 100.00% 1!1O

5000 115 52 78 'T-i-p-r

Lrp-rr^ 11.20 11.40 11.60 11.80 12.00 ' ' ' I ' ' ’ ' I ' ' ' ' I ' ' ' ' I ' ' ‘ ' I ' ' ' ' I ' ‘ ' I ' ' ' ' I ' ' m/z 151.90 61.04% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1$0

5000 115 ' I ' I 78 11.20 11.40 11.60 11,80 12.00 52 m/z 115.00 . 36.28%

TiZz-> 30 35 40 50 60 70 80 90 100 110 120 130 140 150 160 3. Abundance #9592: Benzene-1.2,3.4-44-, 5,6-dichloro- ----- 1$0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 "inTz 78.05 . 20.46%

35 87 I-------- --- - I - -J TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance . #10129: Benzenamine, 2-methyl-4-nrtro- T T - ^77. -106 — -152tT-^ 1 t.20'?i 1:40-1 i:60~i i:8o~i2:oo~ -myz“—52.00 ■ 17.12%

5000 51 ■94'-^-----

T-r-p-T-rr-p-r-n-f-T 1 66 T I'''' I T iiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

23698.D NP091101.M Tue Oct 16 15:10:00 2001 Page 5

' NYC-Wfc_600089156

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NYC-WTC_000089156Source: NYC Law Department, mirrored locally

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