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GC/MS analysis report, sample AD23698, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23698 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089144–000089157

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089155
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1501\23698.D Vial: 11 Acq On : 15 Oct 2001 9:58 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.76 1.00 ug/1 95621 1,4-Dichlorobenzene-d4 11.76

Hit# Of 5 'entative ID MW MolForm CAS# Qual

1 2-Pentai^ne, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 42 2 Propan^ 1- (1-raethylethoxy) - 102 C6H14O 000627-08-7 9 3 Aceto^ 58 C3H6O 000067-64-1 9 4 But^e, 1-ethoxy-________________ 102 C6H14O • 000628-81-9 9 Abundance ' Scan 296 (7.761 min): 23698.D (-) m/z 42.95 100.00% 4(3

59 5000

101 740 7.60 7.80 8.00 8.20 ................................. 3^ Il 11''' ' I Tn/z 59705 53.08% I ' ‘ ' I ' ' ' ' I ‘ ‘ ' I ' I ' ' ' ’ I ' ' ' ' I ' ■n^-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275; 2-Pentanone. 4-hydroxy-4-methyl- 4(3

5000 59 740 7.60 7.80 8.00 8.20 -m/z 100.95 22.00% 15 31 83 ■l-rT-i-p-rJk-rTT-rTvJ^^ ' ' ' I' ' I I '“'“'“'“I I I i ' I I ........ 111' • 11'' 111 Ti/z->________ 10 20 30 40 5() 60 70 80 90 100 110 Abundance #1779; Propane, 1-(1-methylethoxy)- 43 -7— 7 40 7.60 7.80 8.00 8.20 5000 m/z 58.05 18.85%

57 73 87 27 A.r ' I ' ' ' ' I ' Ti/z->________ 10 20 30 40 50 60 70 80 90 100 • 110 Abundance #94: Acetone ____________________ .43 ^7-40 —■7.60 —^7.80 —8.00—8.20- -m/z---- 4-1-05------ “8“^

5000 15 ■58’ 27 ' ' ' I ' ' ' ' I nZz-> 10 20 30 40 50 60 70 80 90 100 110 : 7.40 7.60 7.80 8.00 8.20

23698.D NP091101.M Tue Oct 16 15:09:58 2001 Page 4

NYC-WTC_000089155

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NYC-WTC_000089155Source: NYC Law Department, mirrored locally

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