GCMS analysis results, sample AD25605, Nov 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\NOV1601\25605.D Vial: 22 Acq On : 17 Nov 2001 11:31 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.68 2.41 ug/1 381840 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 'entative ID MW MolForm CAS# Qual 1 2-Pent ano: , 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 72 2 Acetone > 58 C3H6O 000067-64-1 9 3 5-Hexeny2 -one 98 C6H10O 000109-49-9 9 4 MorphoJ/ine, 4-methyl- 101 C5H11NO 000109-02-4 9 '\bundance Scan 287 (7.683 min): 25605.D (-) m/z 43705 100.00% 4^

5000 59

101 ...................... ■ I I , I , , 1 r I I' I I I I I 1

83 7.40 7.60 7.80 8.00 3^ I 53.,. 70 ‘ I ' ' ' ' I ' ' ' ' I ' I ' ' I'l I ' • I ' ' I ■'■ ■ ■ I ■ ■ ' I I I ■ ■ ■ I mTz 59705 :47.88%

L ■nfe-> 10 20 30 40 50 70 60 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 4^

5000 ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ‘ ‘ ' T' ' ' ' 59 7.40 7.60 7.80 8.00 m/z 101.05 22.96% 15 31 101 I I 83 ' I ' ‘ ' I ' nr^ ■-r+ I I ' ' ' ' I ' ' ' ' I ■' ' ' I ' nfe-> 10 20 30 40 60 70 80 90 100 110 ^bundance #62326: Acetone 40 ' I ' ' ' ' I ' ' ' ' I ' r-ri^n-i-r 7.40 7.60 7.80 8.00 5000- m/z 58.05 19756% 58

7i/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205:5-Hexen-2-one ' ' ' I ' ' ' I ' ' ' ■T' ' 40 7.40 7.60 7.80 8.00 m/z 41.05 6.92% 5000

55 38 , 50 I 83 98 ry-i—I—1—ry-i—r-r-r-1— ' I ' ' ' ryn—TT-ry-T-r-rT—f-rS—r-r-r-t—|—r-r-i—r-[— T1^-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

25605.D NP103001.M Wed Nov 28 14:19:05 2001 Page 1

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