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GCMS analysis results, sample AD23948, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23948 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067675–000067689

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23947-D vial: 14 Acq On : 18 Oct 2001 2:00 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.61 ug/1 153416 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pent ano: , 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 64 2 Acetic id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 3-Hydre^ -3-methyl-2-butanone 102 C5H10O2 000115-22-0 17 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 ^bundance Scan 295 (7.747 tnin): 23947.D (-) m/z 42.95 100.00% 40

59 5000- 101 7.40 7.60 7.80 8.00 __________ 38.11 83 I ' ' ' ' I ' ' ' ' I ' ' ' ' r' m/^ 59.0,5 51.96% Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245:2-Pentanone, 4-hydroxy-4-methyl- 40

5000 59 ' ' I ' ' ' ' I ‘ ' 7.40 7.60 7.80 8.00 m/z 101.05 21.38% 31 83 101 I I, 73 '-r+ "■I 70 ' Tife-> 10 20 30 40 50 60 80 90 100 110 Abundance #3292: Acetic acid. 1.1-dimethylethyl ester 40 I" 7.40 7.60 7.80 8.00 50X5 57 m/F" 58.05 16.49% 101

Tife-> 10 15 20 27 30 ~‘ ‘ I

40 ' t 1 I [— > 1 ■ I I I 1

50 60 I ■ I 1 r—1—I—1 I r

70 80 .... T... 90 100 110 Abundance #1697:3-Hydroxy-3-methyl-2-butanone ‘ I ' ' ' ‘ I ‘ ' 50 7.40 7.60 7.80 8.00 m/T” 41.05 6.91%

5000 43 31

...J__ 3§_k I ' * ' ' I ' * * ‘ I ' ' ' ' I ' ' I ' ' '''I w......,. y ........ Tl/z-> 10 20 30 40 50 60 to’ " m" "do" ' ioo " ii6 7.40 7.60 7.80 8.00

23947.D NP101901.M Wed Oct 24 ll:20':42 2001 Page 5

NYC-WTC_000067687

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NYC-WTC_000067687Source: NYC Law Department, mirrored locally

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