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GCMS analysis results, sample AD23993, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23993 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067690–000067704

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23948.D Vial: 15 Acq On : 18 Oct 2001 2:58 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ***************************** * *** *■* ** * ****** * * * * * * * * * *************** *

Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.62 ug/1 154021 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic acid , 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 28 3 Acetone/ 58 C3H6O 000067-64-1 12 4 3-Hyd:^g^-3-methyl-2-butanone 102 C5H10O2 000115-22-0 12 Abundancec Scan 296 (7.754 min): 23948.D (-) m/z 42795 100.00% 43

59 5000

101 -rT-p-!-r-rT-T-F=!4-4?=^^ 740 7.60 7.80 8.00

T,fe-> 10 20 30 36 I, 40 50 II, 60 .......... 70 80 90 100 110 m/z 59.05 55.17% Abundance #64274:2-Pentanone. 4-hydroxy-4-methyl- 4(3

5000 59 7.^ 7.ot' 7.TO"s.OO m/z 58.05 19.92% 101

Tife-> 10 20 27

30 11 40 K) ^-4 60 70 80 83 90 100 110 Abundance #3292: Acetic acid. 1.1-dimethyiethyl ester 43

7.40 7.60 7,80 8.00 5000 57 m/z 101.05 19.34% 101 15 27 T I TiZz-> 10 20 30 40 '' 60 ' ‘ 70 ' "eb" "90" ' i66 " i-io ^bundance #62322: Acetone 43 740 7,60 7.80 8.00 m/^ 41.00 7.44% 5000 58 27 -I............... ■|I"M * I'M I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I Tlfe-> 10 20 30 40 50 60 70 80 90 100 110

23948.D NP101901.M Wed Oct 24 11:22:04 2001 Page 5

NYC-WTC_000067702

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NYC-WTC_000067702Source: NYC Law Department, mirrored locally

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