GCMS analysis results, sample AD23993, Oct 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23948.D Vial: 15 Acq On : 18 Oct 2001 2:58 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.62 0.54 ug/1 51344 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 :ntative ID MW MolForm CAS# Qual 1 1,4-Diehl •obenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-/ ,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 32 3 Benzal ^Shyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 Benze: imine, N-methyl-4-nitro-_____ 152 C7H8N2O2; 000100-15-2 9 ^bundance Scan 717 (11.619 min): 23948.D (-) Tm/z 149.90 100.00% 1$0

5000 115 52 78 11.11.40 11S) 11'to 12.00 .. ............ I........ TVi I I 1 1 1 j I 111 J I I I 1 J I I I I j I ill I 1 1 I I j I l l I I I I I 4^ m/z 151.90 67.01% Tife-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 I ' ' ' ' I ' ‘ T-r-y-r-r

78 11.TO 11.40 11.60 11.80 12.00 52 m/z 115.00 38.22% 35 T TiZz-> 30 40 50 60 70 TO 90 100 110 120 130 150 160 Abundance #9592: Benzene-1.2,3,4^, 5,6-dichlcira- liiO T-r-p-r

115 11.23 11.40 U.K) 11.80 12.00 5000 52 78 "m/z 77795 19.73% ft 35 I nfe-> 30 40 50 60 70 80 90 100 110 120 130140 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- 1!i2 11.^ 11.40 11.60 11.80 12.00 "mTz 52.00 16787% 106 5000 53 81

122

•nfe-> 30 .... ,111......... 1.....,?. 136 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00 T-p-TT-r-p-r-r-rj-

23948.D NP101901.M Wed Oct 24 11:22:06 2001 Page 6

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