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GCMS analysis results for sample AD24877, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24877 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000068991–000069002

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24877.D Vial: 4 Acq On : 6 Nov 2001 3:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 108008 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-Dichloa?obenzene-d4 150 C6C12D4 003855-82-1 50 2 Benzene7af72,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 38 3 Benze: ^ine, N-methyl-4-nitro- 152 C7H8N202i 000100-15-2 14 4 Benza< dehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 711 (11.568 min): 24877.D (-) m/z 149.90 100.00% 1!0

5000 115 52 78 3® 87 ‘“'i' I'''' I I' ‘‘ I m/z 151.90 66.95% TiZz-> 20 30 40 50 60 70 80 90 100,110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 150

ax» 115 . I Q.,,/y.... I, 78 11.20 11.40 11.60 11.80 52 m/z 115.00 37738% 35 mZz-> "40' ’' OT ' I ‘ 1'''' 1 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3.4-d4-, 5,6-dichlora- 1!0

115 11.20 11.40 11.60 11.80 5000 52 78 m/z 78.05 . 18.34%

35 87 I I ‘ I ‘ ‘' I' 11 ■ ■ • 1 ■ • • ■ 1'' ‘ • I'' m^-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10120: Benzenamine, N-methyI-4-nitro- T T 1$2 11.20 11.40 11.60 11.80 m/z 52.00 17708% 77 122 110 5000 65 30 94 46 ll..,..llll... I,l„l,lll.l,. '' 1 ’ ‘ ‘ 1' ‘ ‘ ‘ I '' I' ' I' ‘ ‘' 1''' n' ‘M ‘ ‘ mfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11,20 11.40 11.60 11.80

24877.D NP103001.M Mon Nov 19 08:59:39 2001 Page 3

NYC-WTC_000069001

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NYC-WTC_000069001Source: NYC Law Department, mirrored locally

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