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GCMS analysis results for sample AD24877, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24877 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000068991–000069002

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24877.D Vial: 4 Acq On : 6 Nov 2001 3:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPC3IEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 3-Hydroxy-2-pentanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 7.71 0.52 ug/1 102640 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hydroxy-2-^ntanone 102 C5H10O2 003142-66-3 43 2 2-PentanonaS 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 38 3 4-Hydro; /3-hexanone 116 C6H12O2 004984-85-4 17 4 5-Hexen -one 98 C6H10O 000109-49-9 9 Mxjndance • Scan 291 (7.712 min): 24877.D (-) m/z 42.95 100.00% 4^

59 5000

101 7^ 7.io ‘7^6 “aoo' “ ‘ 36, I T 71 83 + m/z 59.05 52.66% Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #1691:3-Hydroxy-2-pentanone 311 59

5000 45 7'40 Zro' 7.^ 8.00 15 m/z 101.05 20.31% ...I..... II..... ' I ' ‘ ' I ' ' ' ' 1 ' ' ' ‘ I ' n* I, 73 84 102 mfe-> 10 20 30 40 50 60 70 80 9Q 100 110 120 Abundance #64274:2-Penlanone. 4-hydroxy-4-methyl- 4)3 ' '7.^ 7.60 7.80 8.00 5000 m/z 58.05 16.54% 59

27 101 ,,,~l, ,1, 83 .......... ,■■■■■■ mfe-> 10 20 30 40 50 60 70 80 90 100 110 120 Abundance #3241:4-Hydroxy-3-hexanone .. 11 /.11 mA 1111111 5)9 ' ' 7.^' 7.60 7.80 8.00 m/z 41.05 7.73% 31 5000

I 87 116 ' I ' ' ' ' I ' ' ‘' I ' 11 ■ ■' ■ I ■ ■ ■ • I • • ■ ■ I • ' I ' ' ' ' I ‘ ' I ' nnZz-> 10 20 30 40 50 60 70 80 90 100 110 120 7.40 7.60 7.80 8.00

24877.D NP103001.M Mon Nov 19 08:59:37 2001 Page 2

NYC-WTC_000069000

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NYC-WTC_000069000Source: NYC Law Department, mirrored locally

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