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GCMS analysis results for sample AD24696, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24696 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068838–000068852

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPC3IEM\1\DATA\NOV0501\24697.D Vial: 16 Acq On : 6 Nov 2001 2:35 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanone, 2-methyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.32 0.44 ug/1 72495 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanon^ 2-methyl- 100 C6H12O 000565-69-5 72 2 3-Hexanone' 100 C6H12O 000589-38-8 72 3 2,4-Pent^edione 100 C5H8O2 000123-54-6 46 4 Butane,/2,2-dimethyl- 86 C6H14 000075-83-2 33 Abundance 7 4(3 Scan 138 (6.315 min): 24697.D (-) 57 m/z 43.00 100.00% 71

5000 100 jy 6.00 'eJffl' 6.^ 6.60 "n* 3^ 51 85 4^ ' I ■ “ 111... 1.1.1111 fl J111111111) 111111.111 “ “ I.. 111." 11" 111" " 111 “ I “.. J1111111 “ 111 +Tprr^ -h-r TTp m/z 57.00 96.16% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63398:3-Pentanone. 2-methyl- 5(7 43

5000 ' ' I ' ' ' ' I 100 6.00 6.40 6.60 71 m/z 71.00 70.49% 85 ''' 1" " 1 “ " P " ‘ I" " 1" ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance

29 43 #1528:3-Hexanone 57

71 ‘ II 6.00 m/z 100.05 6.20 7™, 6.40 6.60 39.18% 5000 100

TrrrrTTyrmj 4..,n..,..... +TTTyrTTTJ■ TiZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63324:2,4-Pentanedione 43 6.00 6.20 6.40 6.60 "m/z 41.05 22.60% 552 85 100

58 72 +t +TTTT 6.00 6.^ 6.40 6.^ Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105

24697.D NP103001.M Tue Nov 13 12:05:32 2001 Page 1

NYC-WTC_000068846

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NYC-WTC_000068846Source: NYC Law Department, mirrored locally

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