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GCMS analysis results for sample AD23993, Oct 2001

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Laboratory report documenting GCMS analysis of sample AD23993 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067720–000067734

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C:\HPCHEM\1\DATA\OCT1701\23994.D Vial: 16 Acq On : 18 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.49 ug/1 46105 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-HexanQjHfe 100 C6H12O 000589-38-8 86 2 3-PentMone, 2-methyl- 100 C6H12O 000565-69-5 47 3 Butan^ 2,2-dimethyl- 86 C6H14 000075-83-2 42 4 2,4 -^ntanedione 100 C5H8O2 000123-54-6 38 Abundance / Scan 146 (6.378 mln): 23994.D (-) m/z 43.05 100700% 43 57 71 5000 100

6.00 6.20 6.^' 6.60 6.80 T^nJ,ll r'"i + P m/z 57.00 93.74% TiZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1528:3-Hexanone 57

29 71 5000 6.20 ‘ 6.^ ‘ 6.60 " 6.80 6.00 100 m/z 71.00 60.86% TTTTTTT+- prrrtT TiZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #63398:3-Pentanone. 2-methyl- sjz 43 6.00 6.20 6,40 6,60 6.80 5000 m/z 100.05 33773%

L 100 71 85 +rTTrr >> >1 i|< .. . trrrprrrp TiZz-> 5 10 15 20^ 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #732: Butane, 2,2-<iimethyl- I 43 57 6.006.;a) 6.40 6.60 Iso 71 m/^ 41.05 27.88% 29

jkL 5000

15 ""I""I"" 1“'‘I‘ T* TlZz-> 10 15 20:^30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 166' 6.^' 'bM I.ro' 6.^

23994.D NP101901.M Wed Oct 24 11:24:39 2001 Page 1

NYC-WTC_000067728

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NYC-WTC_000067728Source: NYC Law Department, mirrored locally

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