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GCMS analysis results for sample AD23993, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23993 conducted on October 25, 2001, noting unknown compounds.

NYC-WTC_000067720–000067734

Folder label: “GCMS Scan X 10/4/01 An 10/18/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT1701\23994.D Vial: 16 Acq On : 18 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.48 1.08 ug/1 102307 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone / 100 C6H12O 000591-78-6 91 2 2-Hexano: ; 4-hydroxy-5-methyl-3-pr 172 C10H20O2i 061141-74-0 83 3 2 -Hexano; e, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Oxira:^, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 59 Abundance T Scan 157 (6,479 min):23994.D (-) m/z 42.95 100.00% 43

58 5000

6.^ 6.^ 6.80 37| J 71 85 100 . V,,,,, ,1... 1,,,, I,, _ ,, I, m/z 58.05 52.99% mZz-> 20 30 40 50 60 70 80 90 iob 'iio "i^ w Abundance #63384:2-Hexanone 43

5000 58 6.20 6,40 6,60 6.80 29 “m/z 41.05 16.57% I 71 Ti/z-> 20 30 40 50 60 70 80 90 1(X) 110 120 130 140 Abundance #15807:2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4)3

' '6.2b' 6.^' '6,60 ' '6.80 5000 ■m/z 57700 16737% 58 27

Ti/z-> Abundance l-r-p-rt 20 u 30 40 I ... ,7...,.?.,..,;^ 60 70 80 90 ___100 #11968:2-Hexanone, 4-hydroxy-3-propyI- 110 120 130 140 43 6.20 6,40 6,60 6.80 m/z 100.00 7.93% 58

.1. 5000 29

71 ■ 88... 100 ‘ I'' ‘' I ‘' I' 11 • • • I ■ 140 T»fe-> 20 30 40 50 60 " 70 " sb’" 'so " ioo"i-io" w" w 140 6.20 6.40 6.60 6.80

23994.D NP101901.M Wed Oct 24 11:24:42 2001 Page 2

NYC-WTC_000067729

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NYC-WTC_000067729Source: NYC Law Department, mirrored locally

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