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GCMS analysis results for sample AD24334, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of environmental sample AD24334 with detection of unknown compounds.

NYC-WTC_000068240–000068254

Folder label: “508 GCMS Scan X 10/11/01 An 11/2/01

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Scanned page image, NYC-WTC_000068248
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Confound Report Data File : C;\HPCHEM\1\DATA\NOV0101\24334.D Vial: 10 Acq On : 1 Nov 2001 11:48 pm Operator: 209 GALOS San^jle : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C;\HPCHEM\1\METHODS\NP101901 .M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.33 0.42 ug/1 67469 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexan<.^e 100 C6H12O 000589-38-8 64 2 3-Pent none, 2-methyl- 100 C6H12O 000565-69-5 53 3 2,4-P^l.tanedione 100 C5H8O2 000123-54-6 43 4 Hexane, 2,4,4-trimethyl- 128 C9H20 016747-30-1 38 Abundance Scan 140i(6.327min):24334.D(-) m/z43.05 100.00% 4l3 15|7 71 5000 100 I I

6.00 I I . I .

6.20 I I . AJ . I

6.^ I I I . I I

6.80-^ I . . . I

T +rrTT P ■nZz-> 2025303540^ 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1528:3-Hexanone 43 57

29 71 5000 ‘' 1 ‘ ‘ ‘ ‘ 7 • • • ‘ J > • • * 1 ‘ I * 6.00 6.20 6.40 6.60 100 m/z 71.0,0 65.00%

TiZz-> ^bundance

5000 ............. . +TTTT 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63398; 3-Pentanone. 2-methyl-

43 p

100 JUJ 6.00 m/z 100.05 6.20 L 6.40 ' I ' ’ ‘ ’ I 6.60 38.50% 71

TiZz-> Abundance +r 85 20 25 30 35 40 ^ 50 55 60 65 70 75 80 85 90 95 100 105

43 #63324:2,4-Pentanedione p

6.0) m/F” 6.20 41.05 sk. 6.40 6.60 24.95% 5000 85 100

58 72 pW p 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.66' 6.^' ’6.40' 6.OT

24334.D NP103001.M Wed Nov 07 10:39:15 2001 Page 1

NYC-WTC_000068248

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NYC-WTC_000068248Source: NYC Law Department, mirrored locally

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