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GC/MS analysis results for sample AD23843, Nov 2 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23843 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089397–000089417

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089406
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23843.D Vial: 15 Acq On : 31 Oct 2001 4:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************** *'* ********************* Peak Number 2 ^-Pentanone, 4-hydroxy-4-methy Concentration Rank 10 R.T. EstConc Area Relative to ISTD . R.T. 7.70 0.69 ug/^ 163183 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 fentative ID MW -MolForm CAS# Qua! 1 2-Pent ano; , 4-hydroxy-4-methy1- 116 C6H12O2. 000123-42-2 47 2 Acetic a^ d, cyano-, 1,1-dimethylet 141 C7H11NO2. 001116-98-9 17-. 3 3-Hydro/y -2-pentanone 102 C5H10O2 003142-66-3 9 4 Morpho/ine, 4-methyl- 101 CSHilNO 000109-02-4 9 Abundance Scan 289 (7.696 min): 23843.D (-) m/z4^705 100.00% 4)3

59 5000

101 7.40 7.60 7.80 8.00 37,. I 53., .Tl 1,1........................ in/z 57705 50.20% ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I ' I '' I'"'I'I'l' TlZZ-> 10 20 30 40 50 60 70 80 90 100 110 120 130

_JC Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 7.40 7.60 7.80 8.00 m/z 101.05 27701% 27 101 I I 83 n/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #7666: Acetic acid, cyano-, 1,1-dimethylrfhyl ester 5b ‘

7.40 7.60 7.80 8.00 5000 41 m/z 58.05 18.36%

TT/z-> ................... r^r.rllh 10 20 30 40 50 60 3^ . 70 80 90 100. 110 120 '130 Abundance #1691; 3-Hydroxy-2-pentanone -31 ------- 59--------------- "■ ,.7.40L 7.60 7.80. 8.00—- m/z 41.00 7.71% 5000

15 I ----- 45------

' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 10 20 30 40 'so' 60 7o' . ....... I??,. |7 . . ........ 'i', 'so "9'0" ' ioO " 110 " 120 '' iso 7.40 7.60 hz- 7.80 8.00

23843.D NP103001.M Thu Nov 01 14:44:06 2001 Page 2

NYC-WTC_000089406

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NYC-WTC_000089406Source: NYC Law Department, mirrored locally

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