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GCMS analysis results for sample AD24642, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24642 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068684–000068695

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068693
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24642.D Vial: 9 Acq On : 5 Nov 2001 7:46 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.08 ug/1 155916 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Pent. me, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 72 2 Morpho;i?rne, 4-methyl- 101 C5H11NO 000109-02-4 9 3 3-Hy^oxy-2-pentanone 102 C5H10O2 003142-66-3 9 4 Oxiyane, [(1-methylethoxy)methyl]- 116 C6H12O2 004016-14-2 9 Abundance Scan 288 (7.685 min); 24642. D (-) m/z 42.95 100.00% 413

5000 59

101 83 7.40 7.60 7.80 8.00 311 49 m/z 'I ■ ' 'I '-''I I ' ' ' ' I ' ' ' ' I '■ I ' I ' ' ' I I ' ' ' ' I 59.05 47.00% Tl/z-> 10 20 30 40 50 60 70 80 100 110 Abundance #64275; 2-Pentanone. 4-hydroxy-4-methyl- 40

5000 59 7.40 7.60 7.80 8.00 m/z 101.05 19774% 101

L 15 31 ........ 1, I I ,,,, n-+ ' ' ' I ' ''I TlZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4)3

7.40 7.60 7.80 8.00 5000 m/z 58.05 19.73% 101 15 71 27 I 56 I ’ I I I ' • I ■ ■ I ■ I . . . ■ I t - I ■ I ' . ■ ■ I ■ . . . 1 ■ • ■ ■ I Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 21 59 7.40 7.60 7.80 8.00 m/z 41.05 6.91%

5000 45 15 , , I...... I, I..... I ' ' ' ' I ' ' ' ' I ' ' ' ' I . 66 Hj-nr-r-ryrh- 73 84 ' 1 ' ‘ 102 ‘ 1 ' ' ’ ' I ' ' ' ' I Tl&-> 10 20 30 40 50 60 70 80 90 100 110 7.40 ' ' 7.60 ' ' 7.80 ' ' 8.00

24642.D NP103001.M Fri Nov 09 12:20:53 2001 Page 2 NYC-WTC_000068693

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NYC-WTC_000068693Source: NYC Law Department, mirrored locally

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