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GCMS analysis results for sample AD24879, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24879 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069015–000069026

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000069025
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24879.D Vial: 22 Acq On 6 Nov 2001 9:25 am Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 • 1,4-Dichlorobenzene-d4 Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.54 ug/1 95689 1,4-Dichlorobenzene-d4 11.72 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-Dichlorobea!fzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-l,2^X^4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 37 3 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 4 lH-PyrroA[2,3-b]pyridine-2,6-dione 152 C7H8N2O2 017384-56-4 9 flibunSnee-Tx 712 (11.578 min): 24879.D (-) m/z 149.90 100.00% 1$0

5000 115 52 78 40 11.20 11.40 11.60 11.80 12.00 I' ’ •' I I' •I m7FT5T79A7"6T7^3% 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1(0

5000 115 T 78 11.20 11.40 11.60 11.80 1200 52 m/z 114.90 33.51% 35 I ’ • ‘ • I nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2.3,4-d4-, 5,6-ciiohloro- 1!i0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 77.95 19.20%

87

Tife-> 30 35 I 40 50 '' 1 ‘' I' ' 60 70 I ' I'''' I' 80 90100 110 120 130 A T MO AUtt- 150 160 Abundance #66892: Benzaldehyde, 2-hydroxy-3-methoxy- ....... 112 11.^’ ‘1146' 11.TO 'iiiab' 12'00 m/z 52.00 . 18.52% 106 5000 53 81

122 ' I ‘' I'''' I' I ‘ 1'''' I'' • • I'' ‘' I'' mA Am p I T ■nfe-> 30 40 50 60 70 80 90 100 110 120 130l' 'l40 150 160 11.20 11.40 11.60 11.80 12.00

24879.D NP103001.M Mon Nov 19 09:17:20 2001 Page 3

NYC-WTC_000069025

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NYC-WTC_000069025Source: NYC Law Department, mirrored locally

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