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GC/MS analysis report, sample AD23798, Nov 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23798 showing detection of unknown compounds on November 1, 2001.

NYC-WTC_000089299–000089310

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089308
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT3001\23798.D Vial: 9 Acq On : 30 Oct 2001 10:20 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 0.85 ug/1 220447 1,4-Dichlorobenzene-d4 11.71

Hit# Of 5 intative ID MW MolForm CAS# Qual

1 2-Pentanone, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic^^id, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 AceticZacid, cyano-, 1,1-dimethylet 141 C7H11NO2I 001116-98-9 17 4 Acet^e 58 C3H6O 000067-64-1 io Sundance Scan 289 (7.701 min): 23798.D (-) m/z 42795 100.00% 4{3

59 5000 101 7.40 7.60 7.80 8.00 71 83 m/z 59.05 54.08% TiZz-> 10 20 30 40 50 60 80 70 90 100 110 120 130 Abundance #64275; 2-Pentanone, 4-hydroxy-4-methyl-

5000 59 .. __ J 7.40 7.60 7.80 8.00 m/z 101.05 25.35% 15 31 VrTTTVT-rnSTTT-,-rT*^^ 101 I . ............ I 1-n-p-r^ 10 20 30 40 50 60 70 80 90 100 110 120 130 ^bundance _______ #3292:. Acetic acid,-1,1-dimethylethyl ester- 4b 7.40 7.60 7.80 8.00 5000 57 m/z 58.05 18.04% 101

-----177"?" '40 ’ '50' ' TiZz-> 10 20 30 60 70 80^ 90 100 110 120 130 Abundance #7666: Acetic acid, cyano-, 1,1-dimethylethyl ester : ' '-I -' 7'.'- !-'■ . ■_"=_5l9_- . ■ .^7.40=7.60 =7.60= 8.00—- m/z, 41.05 8.21%

5000 ___ 68 126 ■' I ' ' I ' ' ' ' I ' ' ' ' I ' 10 20 30 40 50 60 70 80 90 100 110 120 130 7.40 7.60 7.80 8.00

23798.D NP103001.M Thu Nov 01 12:05:02 2001 Page 2

’ NYC-WTC_000b89308

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NYC-WTC_000089308Source: NYC Law Department, mirrored locally

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