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GCMS analysis results for sample AD24431, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24431 conducted on November 7-9, 2001, identifying unknown compounds.

NYC-WTC_000068413–000068431

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24431.D Vial: 11 Acq On : 3 Nov 2001 12:46 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.55 ug/1 76683 1,4-Dichlorobenzene-d4 11.71

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-DichlQa/6benzene-d4 150 C6C12D4 003855-82-1 91 2 Benzene;;^2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 45 3 2-AdatBdntanone 150 C1OH140 000700-58-3 23 4 Acenaphthylene _____________________________ 152 C12H8 000208-96-8 10 Abundance Scan 712 (11.579 min): 24431 .D (-) m/z 149.90 100.00% 1!>0

5000 115

52 78 11 20 11.40 11.60 11.80 12.00

TiZz-> 30 40 50 I I 60 64 .,.41,.%...... 70 80 90 100 110 120 130 140 150 160 m/z 151.90 62.42% Abundance #9593:1.4-Dichlorobenzene-d4 1$0

5000 115 78 11 20 11.40 11.60 11.80 12.00 52 m/z 115.00 ^7724%

nfe-> 30 35 40 50 60 70 ..J..." 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1!i0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 77.95 . 18.16%

tVz-> 30 35 I 40 50 ...... II,,. A.......... 1,1......... 60 70 80 90 100 110 120 130 140 150 160 Abundance #9842:2-Adamantanone Ito 11 20 11.40 11.60 11.80 12.00 m7z 52.00 . 13.63% 79 5000

72 93 104 117 ill I 132 ■n/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24431.D NP103001.M Tue Nov 13 10:06:33 2001 Page 6

NYC-WTC_000068426

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NYC-WTC_000068426Source: NYC Law Department, mirrored locally

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