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GCMS analysis results for sample AD24431, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24431 conducted on November 7-9, 2001, identifying unknown compounds.

NYC-WTC_000068413–000068431

Folder label: “GCMS Scan X 10/12/01 An 11/3/01

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Scanned page image, NYC-WTC_000068425
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0201\24431.D Vial: 11 Acq On : 3 Nov 2001 12:46 am Operator: 209 GALOS Sample : gc/ms unknown Inst ! GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.72 ug/1 237392 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pentanoner; 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 53 2 Acetic adid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Morpljoline, 4-methyl- 101 C5H11NO 000109-02-4 9 4 3-Hydroxy-2-pentanone 102 C5H10O2 003142-66-3 9 ftbundanc^ Scan 288 (7.686 min): 24431 .D (-) m/z 47795 100.00% 4(3

59 5000

101 7.40 7.60 7.80 8.00 .. . ..,.. .?,N I •' • 11 • ■ • ■ I ■ ■ • ■ I ■ 53.,. ' I ' ''If I ' 71 I I ‘ 83 ' I '' ' ' I ' I I I ■ ■ ' I ' m/z syToT 53.20% ■nfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64274:2-Pentanone, 4-hydroxy-4-methyl- 4(3

5000 59 7.40 7.60 7.80 8.00 m/z 100.95 21.98% 27 101 I I 83 ...... ... Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292; Acetic acid. 1,1-dimethylethyl ester 4(3 ....... .......... 7.40 7.60 7.80 8.00 5000- 57 m/z 58.05 17791% 101 15 27 ''i I I I I ' I I ' I ' ' I I I ' ' ' ' I I 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4|3 7.40 7.60 7.80 8.00 m/z 41.05 7.59% 5000- 101 15 71 I Xh 27 I 56 I ■ I I I ’ ' I ■ ' I ■ I • ' ' ' I I • ' ■ I ■ ■ I ■ I ■ ■ I ■ I ■ ■ ■ ■ I I ...

nfe—> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24431.D NP103001.M Tue Nov 13 10:06:31 2001 Page 5

NYC-WTC_000068425

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NYC-WTC_000068425Source: NYC Law Department, mirrored locally

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