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GCMS analysis results for sample AD24947, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24947 conducted on November 19, 2001, noting unknown compounds.

NYC-WTC_000069095–000069105

Folder label: “GCMS Scan X 10/18/01 An 11/6/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0601\24947.D Vial: 15 Acq On : 7 Nov 2001 2:25 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.53 ug/1 99035 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 l,4-Dichloroh<^nzene-d4 150 C6C12D4 003855-82-1 47 2 2-Adamantan^e 150 C1OH140 000700-58-3 23 3 Benzene-l,/,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 22 4 Benzoic q^id, 2,5-dimethyl-___________ 150 C9H10O2 000610-72-0 9 Abundance Scan 712 (11.580 tnin): 24947.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 11.20 11.40 11.TO 11.80 12.00 4^ m/z 151.90 70.82% iTife-> 30 40 50 60 70 TO 90 100 110 120 130 140 150 IK) Abundance #9593; 1,4-Dichlorobenzene-d4 1$0

5000 115 11^ 1t40 1?.6O 11'to IZOD 52 78 m/z 115.00 38.39%

■nh-> 35 '30'" 40 „l... II,.,?,, 50 TO 70 TO 90 100 110 120 130 140 150 160 I ' ' ‘ ' I ■•V

Abundance #9842:2-Adamantanone liO

79 11J20 11.40 11.60 11,80 12.00 5000 m/z 78.05 18.92%

93 104 If 11 132 ■T^ TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3,4-d4-, 5,6<lichloro- ' 1 ‘ ‘ I ' ' liiO 1120 11.40 11.60 11.80 12.00 m/z 52.00 . 14.86% 115 5000 52 78

87

n&-> 35 I ' I'''' I' ‘ ‘' I 30 40 50 ‘‘ I 60 ' I' 70 I I'''' I ‘ 80 90 A 100 110 120 130 140 150 160 .... ............ I • ( . I . -ri-. I . I 1 I . • . I . 11.20 11.40 11.60 11.80 12.00

24947.D NP103001.M Fri Nov 16 15:00:46 2001 Page 2

NYC-WTC_000069104

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NYC-WTC_000069104Source: NYC Law Department, mirrored locally

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