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GCMS analysis results, sample AD23909, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067555–000067578

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data Pile : C:\HPCHEM\1\DATA\OCT1801\23909.D Vial: 4 Acq On : 18 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 1,4-Dichlorobenzene-d4 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.63 0.52 ug/1 48957 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 T^tative ID MW MolForm CAS# Qual 1 1,4-DichlQr^benzene-d4 150 C6C12D4 003855-82-1 53 2 2 -Adaman^none 150 C10H14O 000700-58-3 32 3 4-Amino^-chlorobenzonitrile 152 C7H5C1N2 020925-27-3 14 4 Benzejfe-l,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 12 Abundance Scan 718 (11.630 min): 23909.D (-) m/z 149.90 100.00% 1!i0

5000 115 52 78 40 11.20 11.40 11.60 11.80 12.00 tX ■

UrrTT+i-r m/z 151.85 62717% TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593; 1,4-Dichlorobenzene-d4 1$0

5000 115 T-y-r-r-j-r-p-r 78 11.20 11.40 11.60 11.80 12.00 52 m/z 115.00 34.54% 35 TiZz-> 30 40 50 60 70 «) 90 100 110 120 130 140 150 160 Abundance #9842:2-Adamantanone liiO

79 11.20 11.40 11.60 11.80 12.00 5000 “mTz 78705 17.31%

54 72 93 104 117 pX I'.l...... I......... 'h 132 I T '' ‘' I Ti&-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10110; 4-Amino-2-chlorob8nzonitrile 1!i2 11.20 11.40 U.K) 11,80 1200 “m/z 52.00 16.13% 5000

zw, 90 117 125 76 I TT-p-r I ‘ ‘‘ I ' ' I ‘ ' Tlfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 1160 11.80 12(n

23909.D NP091101.M Fri Oct 19 10:17:11 2001 Page 6

NYC-WTC_000067568

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NYC-WTC_000067568Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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