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GCMS analysis results, sample AD23909, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067555–000067578

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23909.D Vial: 4 Acq On : 18 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 5 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 2.05 ug/1 192175 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 'entative ID MW MolForra CAS# Qual 1 2-Penta: me, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic/ cid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 3 -Hy^oxy- 2 -pentanone 102 C5H10O2 003142-66-3 9 4 Morpnoline, 4-methyl- 101 C5H11N0 000109-02-4 9 bundance-' Scan 295 (7.747 min): 23909.D (-) m/z 42795 100.00% 4)3

SOX)

10 20 30 40 + 50 60 59

71 70 80 83 90 101

I 1 ' - ' ' I 100 110 7^ m/z 7.^ 59.05 L 7.^ 8.00 49.68% Abundance #64275; 2-Pentanone. 4-hydroxy-4-methyt- 4i3

5000 K' 59 7.40 7.60 7.80 8.00 m/z 101.05 20.78% 15 31 101 T-r-r-r-ir ( I ' “ I ”’ ' ' ' 1 ‘

■nfe-> 10 20 30 40 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester

7.40 7.60 7.80 8.00 5000 57 m/z 58.05 15.94% 101

TiZz-> ‘ 'lb' " 27 ’ 30 •I* I ' I ' ' ' ' I ■ ... I . I I . I ... I I .... I . ... I 40 50 60 70 80 90 100 110 Abundance #1691:3-Hydroxy-2-pentanone 31 59 7.40 7.60 7.80 8.(X) m/z 41.05 6760%

500)

, T , I..... 10 20 30 40 rRr.,.|l|^ 50 60 ‘ 70 73 "ao“ 64.............. 102 “ iro " iio ■ 7.40 7.60 7.80 8.00

23909.D NP091101.M Fri Oct 19 10:17:09 2001 Page 5

NYC-WTC_000067567

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NYC-WTC_000067567Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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