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GCMS analysis results, sample AD23910, Oct 2001

Machine-extracted title · confidence 85%

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

NYC-WTC_000067579–000067600

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23910.D Vial: 5 Acq On : 18 Oct 2001 8:06 pm Operator: 209 GALOS San^le : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************************************. Peak Number 4 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.75 1.36 ug/1 123101 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentan e, 4-hydroxy-4-methy1- 116 C6H12O2 000123-42-2 53 2 Acetic cid. 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Acetone 58 C3H6O 000067-64-1 10 4 5-Hexen-2-one 98 C6H10O 000109-49-9 9 Abundance Scan 295 (7.753 min): 23910.D (-) m/z 42.95 100.00% 4)3

59 500)

101 7.40 7.60 7.80 8.00 83 I ' ' ‘ ' 1 ‘ ' I ‘ I ' ' ' * I ' ‘ ‘ ' I m/z 59?^ 52.35% 10 20 30 40 "5^ «) 70 80 90 100 110 M)undance #64275:2-Pentanone, 4-hydroxy-4-methyl- 40

5000 .......... 59 7.40 7.«) 7.80 8.00 m/z 101.05 21.44% 15 31 101 I I I 83 TiZz-> 'io 20 '30' ' ' ' I-' I ' ' ‘ ' I ' ‘ ' I ' ‘ ‘ ' I ' 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester

" I ■ ■ " N ■ TT-p-n-T-p- 7.40 7.60 7.80 8.00

* "I 5000 57 18.89% 101 15 I 27 I .................... I , TiZz-> 10 20 30 40 60 70 80 90 100 110 Abundance #62322: Acetone 4|3 7.40 7.OT “ 7.ro " aoo' “ ' ‘ m/^ 41.00 8.58% 500) 58 27 I ■ ■ I ' ' ' * I ' ' ‘ ' I . . I I f I I I I I • f I I ( I I I . I . . I I • I ' ' ' ' I ' ' ' “ I ' ' ‘ ' I 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

23910.D NP091101.M Fri Oct 19 10:18:07 2001 Page 4

NYC-WTC_000067590

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NYC-WTC_000067590Source: NYC Law Department, mirrored locally

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