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GCMS analysis results for sample AD24492, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24492 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068634–000068646

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0501\24492.D Vial: 8 Acq On : 5 Nov 2001 6:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 11.57 0.53 ug/1 95020 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlorobenzene-d4 150 C6C12D4 003855-82-1 53 2 Benzene-l^Z;3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 27 3 4-Amino22^chlorobenzonitrile 152 C7H5C1N2 020925-27-3 14 4 Acena^hnhylene______________________ 152 C12H8 000208-96-8 10 Abundance Scan 711 (11.572 min): 24492.D (-) 'm/z 149.90 100.00% liiO ft 5000 115

52 78 ■p’

11.20 11.40 11.60 11.80 12.00 t'' HI.I ,'' I'''' 66 I' ,1. 1'1'111'11'l I ■ 111,1, > 1111 I 1111 m/z 151.90 64.48% ■ I ‘' I'' Tl/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000- 115 ......t/V... 11.20 11.40 11.60 11.80 12.00 52 78 m/z 114.90 36764% 35 87 ...■.Jll'l.. Ti&-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3,4-d4-, 5,6-dichloro- liiO

115 11.20 11,40 11,60 11,80 12.00 5000 52 78 m/z 78.05 18.40%

35 87 1 ' I ' ' ' ' I ' ' '' I ' ' '' I ' ' ' ' I' I I '' ' ' I ' — 44^ b/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #10110:4-Amino-2-chlorobenzonittile ' ' ' I ' ' ' ' I ' 1!i2 11.20 11.40 11.60 11.80 12.00 in/z 52.00 14797%

5000

7B 117 125 I ' ‘ H I ‘ ‘ ' I T-r-p-r Tl/Z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24492.D NP103001.M Fri Nov 09 12:19:55 2001 Page 4

NYC-WTC_000068645

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NYC-WTC_000068645Source: NYC Law Department, mirrored locally

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