GCMS analysis results for sample AD24397, Nov 2001

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Library Search Compound Report Data File S Cs\HPCHEM\1\DATA\NOV0201\24397.D vial: 3 Acq On ; 2 Nov 2001 5:00 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 1,4-Dichlorobenzene-d4 Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 11.58 0.50 ug/1 72728 1,4-Dichlorobenzene-d4 11.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 1,4-DichlorobezCzene-d4 150 C6C12D4 003855-82-1 87 2 Benzene-l,2^z3S4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 42 3 Acenaphthy^ne 152 C12H8 000208-96-8 10 4 4-Amino-X-chlorobenzonitrile 152 C7H5C1N2 020925-27-3 10 Abundance Scan 712 (11.578 min): 24397.D (-) m/z 149.90 100.00% liiO

5000 115 78 52 11.^ 11.40 11.60 11.80 12.00 40 Ti/z-> ' ' I • ‘ ' t'l ' ' 30 40 Ann —AVA nA 50 60 70 80 90 100 110 120 130 140 150 160 ra/z 151.90 60.11% Abundance #9593:1,4-Dichlorobenzene-d4 1!i0

5000 115 78 11.^' 'i't4b' 'lYeo 'll to 'izob 52 m/z 114.90 . 36.86% 87 35 nA T 4^ nfe-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 MHindance #9592: Benzene-1,2.3,4-d4-, 5.6-dichloro- Ito 11.^' 'i'i!4o' 'iTeo n^so' 'izob 115 5000 52 78 m/z 78705 20.87%

87

rn/z-> 30 35 I 40 50 60 I ■ I • < 111 ■ ■ I ■ I ■ ■ ■ 11 ■ 70 80 90 100 110 120 A 1' ‘ ‘ ' I 130 140 150 160 Abundance #67015: Acenaphthylene I I I ■ ■ , I , . , Tj . , , .y I ■ ■ H ' 1$2 11.20 11.40 11.60 11.80 12.00 m/z 52.00 13.85%

u 5000

„ 76 63 I 126 . I, I. iH, I, ,?T,, 98 T T TiZz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 11.20 11.40 11.60 11.80 12.00

24397.D NP103001.M Mon Nov 05 12:17:02 2001 Page 2

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