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GCMS analysis results for sample AD24493, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24493 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068647–000068658

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068657
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24493.D Vial; 3 Acq On 5 Nov 2001 1:13 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.57 0.55 ug/1 89270 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 l,4-Dichlo;zJbenzene-d4 150 C6C12D4 003855-82-1 47 2 Benzene;><2/3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 4-Arninjz^-chlorobenzonitrile 152 C7H5C1N2i 020925-27-3 9 4 Acenaphthylene 152 C12H8 000208-96-8 9 Abundance Scan 711 (11.573 min): 24493.D (-) Tm/z 149.90 100.00% 1$0 ft

552

52 78 115 __ i\... 11.20 11.40 11.60 11.80 12.00 40 iVz-> I.,..:.-, 30 40 50 60 70 80 90 100 110 120 rX 130 140 150 160 m/z 151.90 / 56.57% Abundance #9593: 1,4-Dichlorobenzene-d4 1$0

5000 115 ___ l\__ 11.20 11.40 11.60 11.80 12.00 52 78 m7F^j:47yo“~^8TTo% 35 7Vz-> 30 40 50 60 70 80 90 100 110 1 20 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- 1$0

115 11.20 11.40 11.60 11.80 12.00 5000 52 78 m/z 78.05 18.73%

35 87 I I I' ' ' ' I ‘ ' I ' ' ' ‘ I ' ' 44^ Tl/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Sundance #10110: 4-Amino-2-chlorobenzonitrile 152 11.20 11.40 11.60 11.80 12.00 m/z 52.00 14.42%

5000-

63 90 117 125

30 40 50 60 I

70 76 80 90 100 110 120 130 140 150 160 J 11.20 11.40 11.60 11.80 12.00

24493.D NP103001.M Fri Nov 09 12:15:35 2001 Page 3

NYC-WTC_000068657

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NYC-WTC_000068657Source: NYC Law Department, mirrored locally

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